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Type Kim, S.-H.; Lee, J.Y.; Ahn, J.-P.; Choi, P.-P.
  Publication Fabrication of Atom Probe Tomography Specimens from Nanoparticles Using a Fusible Bi-In-Sn Alloy as an Embedding Medium Volume Journal Article
Pages 2019
  Abstract  
  Corporate Author Microscopy and Microanalysis  
Publisher 25  
Editor 2
  Summary Language 438-446 Series Editor atom probe tomography; fusible alloy; nanoparticles  
Abbreviated Series Title We propose a new method for preparing atom probe tomography specimens from nanoparticles using a fusible bismuth-indium-tin alloy as an embedding medium. Iron nanoparticles synthesized by the sodium borohydride reduction method were chosen as a model system. The as-synthesized iron nanoparticles were embedded within the fusible alloy using focused ion beam milling and ion-milled to needle-shaped atom probe specimens under cryogenic conditions. An atom probe analysis revealed boron atoms in a detected iron nanoparticle, indicating that boron from the sodium borohydride reductant was incorporated into the nanoparticle during its synthesis.
  Series Issue ISSN  
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  Expedition Cambridge University Press Notes  
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Serial URL ISBN  
2019/02/04 1431-9276 no NU @ karnesky @ 11534
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