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Grennan-Heaven, N.; Cerezo, A.; Godfrey, T.J.; Smith, G.D.W.
Publication
Optimisation of a scanning atom probe with improved mass resolution using post deceleration
Volume
Journal Article
Pages
2007
Abstract
Ultramicroscopy
Corporate Author
Publisher
107
Editor
9
Summary Language
705-712
Series Editor
3D atom-probe; time-of-flight mass spectrometry; mass resolution
Abbreviated Series Title
In this paper, we present calculations and experimental results obtained using post deceleration of ions in a scanning atom probe (SAP) geometry to improve the mass resolution. Various electrode geometries, tip to electrode distances in the range 50-170 mu m and three different pulse shapes have been evaluated. Experimental mass resolutions of 750 FWHM and 200 FWTM have been achieved reproducibly for the W-184(3+) peak without the use of a reflectron lens. 3D finite element electrostatics software has been used to simulate the ion trajectories through the instrument and thus to calculate the variations in velocities for the different electrode configurations. The observed trends are found to agree well with experimental results.
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URL
ISBN
0304-3991
ISI:000247770100003
no
NU @ m-krug @
9887
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